trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Journal of the American Chemical Society, , vol. 125, # 13 p. 3867 - 3870
in tetrahydrofuran other Radiation; microwave-accelerated preparation of arylzinc bromide by Rieke zinc insertion into aryl bromide under sealed vessel conditions for 10 min; THF 180°C; HLPC or MS;
