4-(乙氧羰基)苯基碘化锌合成路线 （共 24 条）
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.0833333 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
lithium chloride in tetrahydrofuran; toluene T=110°C; 48 h; Schlenk techniqueInert atmosphere;
参考文献
Shirakawa, Eiji; Tamakuni, Fumiko; Kusano, Eugene; Uchiyama, Nanase; Konagaya, Wataru; Watabe, Ryo; Hayashi, Tamio
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 521 - 525
Angew. Chem., 2014 , vol. 126, # 2 p. 531 - 535,5
反应条件
1: 4-ethoxycarbonylphenylzinc iodide With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 5 h; 2: 1,4-Diiodobenzene With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 10 h; 3: With iodine in various solvent(s)
参考文献
Hossain, Kabir M.; Kameyama, Toru; Shibata, Takanori; Takagi, Kentaro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2415 - 2420
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=0°C;
参考文献
MERCK and CO., INC.
Patent: WO2008/156721 A1, 2008 ;
Location in patent: Page/Page column 40 ;
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.25 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 3-diphenylphosphino-2-(diphenylphosphino)methyl-2-methylpropyl acetate in N,N,N',N'-tetramethyl-urea T=20°C; Negishi coupling reaction; 24 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 8 p. 1692 - 1695
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 T=35°C; Substitution; 16 h;
参考文献
Chemistry Letters, , # 11 p. 1241 - 1242
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere;
参考文献
Kim, Seung-Hoi; Rieke, Reuben D.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1984 - 1993
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.166667 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
