4-(乙氧羰基)苯基碘化锌合成路线 （共 24 条）
反应条件
1: 4-ethoxycarbonylphenylzinc iodide With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s)
T=45°C; 5 h;
2: 1,4-Diiodobenzene With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s)
T=45°C; 10 h;
3: With iodine in various solvent(s)
参考文献
Hossain, Kabir M.; Kameyama, Toru; Shibata, Takanori; Takagi, Kentaro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2415 - 2420
反应条件
1: With lithium chloride in N,N-dimethyl-formamide
T=50°C; P=760.051 Torr; 48 h;
2: With hydrogenchloride; water in N,N-dimethyl-formamide
参考文献
Kobayashi, Koji; Kondo, Yoshinori
Organic Letters, 2009 , vol. 11, # 9 p. 2035 - 2037
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi cross-coupling reaction; 0.25 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi cross-coupling reaction; 14 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
