乙基4'-氰基-3-联苯羧酸酯合成路线 (共 5 条)
反应条件
triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane; pentane
参考文献
Tucker, Charles E.; Majid, Tahir N.; Knochel, Paul
Journal of the American Chemical Society, 1992 , vol. 114, # 10 p. 3983 - 3985
反应条件
[bdmim][BF4]; 1-butyl-2-(diphenylphosphanyl)-3-methylimidazolium hexafluorophosphate; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; toluene T=20°C; Substitution; Negishi cross-coupling reaction; 0.3 h;
参考文献
Sirieix; Ossberger; Betzemeier; Knochel
Synlett, 2000 , # 11 p. 1613 - 1615
反应条件
potassium phosphate; cyclohexyl BrettPhos; palladium diacetate in 1,1-dimethylpropan-1-ol T=20 - 110°C; Suzuki-Miyaura reaction; Inert atmosphere;
参考文献
Bhayana, Brijesh; Fors, Brett P.; Buchwald, Stephen L.
Organic Letters, 2009 , vol. 11, # 17 p. 3954 - 3957
反应条件
zinc; tetrakis(triphenylphosphine) palladium(0) 1) THF, rt, 2) THF, rt; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 56, # 4 p. 1445 - 1453
反应条件
n-butyllithium; triphenylphosphine; zinc dibromide; bis(dibenzylideneacetone)-palladium(0) Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 52, # 21 p. 7201 - 7220