1: With 4-methyl-morpholine; isobutyl chloroformate in ethylene glycol dimethyl ether T=0°C; 0.0333333 h; 2: With ammonia in ethylene glycol dimethyl ether; water T=20°C; 1 h; Further stages.;
参考文献
Toumi, Mathieu; Couty, Francois; Evano, Gwilherm
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1270 - 1281
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Belagali, Shiddappa L.; Mathew, Thankamma; Himaja, M.; Kocienski, Philip
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 1 p. 45 - 47
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 0.5 h; 2: With sodium tetrahydroborate; water in tetrahydrofuran T=0°C; 0.5 h;
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Belagali, Shiddappa L.; Mathew, Thankamma; Himaja, M.; Kocienski, Philip
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 1 p. 45 - 47
