3-甲基-CBS-氧硼啶合成路线 (共 731 条)
反应条件
PinP(O)H; [Pd(dibenzylideneacetone)2] in tetrahydrofuran; 1,4-dioxane T=80°C; Kumada Coupling; 22 h;
参考文献
Organic Letters, , vol. 8, # 16 p. 3457 - 3460
反应条件
bis(carbene)-derived nickel(II)-pincer complex in tetrahydrofuran T=20°C; Grignard coupling reaction; 48 h;
参考文献
Synthesis, , # 18 p. 2853 - 2861
反应条件
1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) in diethyl ether T=20°C; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 51 p. 17978 - 17979
反应条件
Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran T=50°C; Kumada-Corriu reaction; 3 h;
参考文献
Tetrahedron, , vol. 63, # 20 p. 4304 - 4309
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 92 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 9 p. 1495 - 1498
反应条件
zinc(II) chloride; 3-Cl-pyridine-Pd-{CH-[N-(2,6-di-iPrC6H3)CH]2}Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=20°C; Negishi cross-coupling reaction; 24 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 18 p. 4749 - 4755
反应条件
1.1: 97 percent / toluene; diethyl ether / 0.5 h / 25 °C 2.1: HCl / H2O; acetone / 0.5 h / 25 °C 2.2: 98 percent / triethylamine / H2O; acetone / 0.5 h / 25 °C View Scheme
参考文献
Tsutsui, Hironori; Ichikawa, Tomoko; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 8 p. 1869 - 1878
参考文献
Olah,G.A. et al.
Journal of the American Chemical Society, 1967 , vol. 89, p. 5259 - 5265