3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C;
参考文献
Duplais, Christophe; Bures, Filip; Sapountzis, Ioannis; Korn, Tobias J.; Cahiez, Gerard; Knochel, Paul
Angewandte Chemie - International Edition, 2004 , vol. 43, # 22 p. 2968 - 2970
反应条件
1: (i), (ii) CrO3, H2SO4 2: (i) CF3CO2H, (ii) H2, Pd-C View Scheme
参考文献
Lednicer,D. et al.
Journal of Medicinal Chemistry, 1972 , vol. 15, # 12 p. 1239 - 1243
反应条件
1: diethyl ether / Erhitzen des Reaktionsprodukts mit Essigsaeure, Acetanhydrid und Naphthalin-2-sulfonsaeure und anschliessend mit Schwefel 2: KMnO4 View Scheme
参考文献
Dauben; Tanabe
Journal of the American Chemical Society, 1953 , vol. 75, p. 4969,4972
参考文献
Bogert; Hamann
Am. Perfumer, 1930 , vol. 25, p. 75
Full Text Show Details
Hardegger; Redlich; Gal
Helvetica Chimica Acta, 1945 , vol. 28, p. 628,633
参考文献
Shoesmith; Connor
Journal of the Chemical Society, 1927 , p. 2232
反应条件
1: With boric acid trimethyl ester in tetrahydrofuran T=20°C; 2: With acidic aq. solution
参考文献
Journal of the American Chemical Society, , vol. 125, # 42 p. 12961 - 12970
反应条件
water in tetrahydrofuran slow addn. of 10 mmol of the Grignard reagent to a stirred soln. of borane in THF (40 mmol); the mixt. was poured into ice-water and acidified with 10percent HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;;
参考文献
Journal of Organometallic Chemistry, , vol. 259, # 3 p. 269 - 274
反应条件
diethyl ether und anschliessenden Hydrolyse;
参考文献
Journal of the American Chemical Society, , vol. 54, p. 4415,4418
反应条件
in tetrahydrofuran dropwise addn. of p-MeOC6H4MgBr to borane at -70°C; stirred below -60°C for 1 h; hydrolyzed (sulfuric acid); filtration; sepn. of org. layer; extn. of aq. layer (ether); combined org. layer washed (H2O); dried (Na2SO4); concn. of soln.; crystn.; washed (hexane, H2O); IR; NMR; mass spectra;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3896 - 3901
反应条件
diethyl ether und anschliessenden Hydrolyse;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>128, p. 153,169,170
