3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 2 h;
参考文献
Amatore, Christian; Jutand, Anny; Negri, Serge; Fauvarque, Jean-Francois
Journal of Organometallic Chemistry, 1990 , vol. 390, # 3 p. 389 - 398
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 81 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Bumagin, N. A.; Luzikova, E. V.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1480 - 1486
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1650 - 1656
反应条件
1: diethyl ether 2: 310 °C / 30 - 40 Torr / Leiten ueber aktiviertes Aluminiumoxyd View Scheme
参考文献
Marvel; Hein
Journal of the American Chemical Society, 1948 , vol. 70, p. 1895,1897
参考文献
Allred,E.L. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 26 - 29
反应条件
1: 4-methoxyphenyl magnesium bromide With titanium tetraethoxide in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: 2-chloro-5-carboxybenzene With tributylphosphine; cobalt(II) chloride in tetrahydrofuran T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Zeng, Jing; Liu, Kun Ming; Duan, Xin Fang
Organic Letters, 2013 , vol. 15, # 20 p. 5342 - 5345
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran -78 deg C, 10 min, 20 deg C, 10 min;
参考文献
Bumagin, Nikolai A.; Luzikova, Elena V.
Journal of Organometallic Chemistry, 1997 , vol. 532, # 1-2 p. 271 - 273
反应条件
anhydrous iron chloride; Ipr.HCl in tetrahydrofuran T=0 - 40°C; 1.66667 h;
参考文献
Ghorai, Sujit K.; Jin, Masayoshi; Hatakeyama, Takuji; Nakamura, Masaharu
Organic Letters, 2012 , vol. 14, # 4 p. 1066 - 1069
反应条件
1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2: n-heptane; dichloromethane / 0.33 h / 20 °C View Scheme
参考文献
Mahoney, Stuart J.; Lou, Tiantong; Bondarenko, Ganna; Fillion, Eric
Organic Letters, 2012 , vol. 14, # 13 p. 3474 - 3477
反应条件
diethyl ether anschliessende Behandlung mit Eis und wss. HCl;
参考文献
Dubinin
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 696,699
J. Gen. Chem. USSR (Engl. Transl.), 1949 , vol. 19, p. 663,666
反应条件
in tetrahydrofuran Reduction;
参考文献
Baciocchi, Enrico; Bietti, Massimo; Salamone, Michela; Steenken, Steen
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2266 - 2270
