3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: in tetrahydrofuran T=-78 - 20°C; 2: With ammonium chloride in tetrahydrofuran
参考文献
AMGEN INC.
Patent: US2010/160280 A1, 2010 ;
Location in patent: Page/Page column 79 ;
反应条件
pyridinium chlorochromate
参考文献
Tobisu; Chatani; Asaumi; Amako; Ie; Fukumoto; Murai
Journal of the American Chemical Society, 2000 , vol. 122, # 51 p. 12663 - 12674
反应条件
1-ethyl-2-pyrrolidinone; 4-(N,N-dimethlyamino)pyridine; phosphonic acid diethyl ester; nickel dichloride; zinc dibromide in tetrahydrofuran T=20°C; 1 h;
参考文献
knochel, Paul; Gavriushin, Andrei; Kofink, Christiane Charlotte; Manolikakes, Georg
Patent: US2010/184977 A1, 2010 ;
Location in patent: Page/Page column 4 ;
反应条件
1-ethyl-2-pyrrolidinone; 4-(N,N-dimethlyamino)pyridine; phosphonic acid diethyl ester; nickel dichloride; zinc dibromide in tetrahydrofuran T=20°C; 48 h;
参考文献
Gavryushin, Andrei; Kofink, Christiane; Manolikakes, Georg; Knochel, Paul
Organic Letters, 2005 , vol. 7, # 22 p. 4871 - 4874
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
C68H72Cl2N6NiP2; water; lithium chloride; zinc(II) chloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada coupling reaction; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 83 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Denmark, Scott E.; Wu, Zhicai
Organic Letters, 1999 , vol. 1, # 9 p. 1495 - 1498
反应条件
1: diethyl ether 2: chromic acid View Scheme
参考文献
Ziegler; Ochs
Chemische Berichte, 1922 , vol. 55, p. 2273
参考文献
Holmberg
Acta Chemica Scandinavica (1947-1973), 1952 , vol. 6, p. 421,425
Acta Chemica Scandinavica (1947-1973), 1956 , vol. 10, p. 591
反应条件
1: tetrahydrofuran / 5.5 h / Heating 2: p-TSA / benzene / 2.5 h / Heating 3: 8.5 percent / aq. NaOH, TEBA / 72 h / Heating View Scheme
参考文献
Singh, Satendra; Meyer, Karen L.; Magarian, Robert A.
Bioorganic Chemistry, 1996 , vol. 24, # 1 p. 81 - 94
