3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether 16 h; Ambient temperature;
参考文献
Pridgen, Lendon N.; Killmer, Lewis B.
Journal of Organic Chemistry, 1981 , vol. 46, # 26 p. 5402 - 5404
反应条件
bis(acetylacetonate)nickel(II); 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran T=20°C; Corriu-Kumada-Tamao coupling; 18 h;
参考文献
Tetrahedron, , vol. 61, # 13 p. 3261 - 3269
反应条件
potassium permanganate; copper(l) iodide 1.) THF, - 30 deg C, 1 h, 2.) Me2CO, 0 deg C,; Yield given. Multistep reaction;
参考文献
Angewandte Chemie, , vol. 104, # 11 p. 1554 - 1556
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 5-Bromothiophene-2-carboxaldehyde With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
参考文献
I.G. Farbenind.
Patent: DE501607 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 2521
反应条件
1: 4-methoxyphenyl magnesium bromide With titanium(IV) isopropylate in tetrahydrofuran; toluene T=-40°C; 0.0833333 h; Inert atmosphere; 2: C10H19ClN2O2 in tetrahydrofuran; toluene T=-40 - 20°C; 4 h; Inert atmosphere;
参考文献
Barker, Timothy J.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8325 - 8328
反应条件
in tetrahydrofuran T=-78°C; 1 h; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
tetrasulphure tetranitride in benzene Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2417 - 2421
反应条件
hydrogenchloride 1.) THF, 66 deg C, 2 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rahman, M. T.; Nur, H. P.
Journal of the Indian Chemical Society, 1994 , vol. 71, # 6-8 p. 469 - 474
参考文献
Baddar; El-Assal
Journal of the Chemical Society, 1951 , p. 431
Full Text Show Details
Baddar et al.
Journal of the Chemical Society, 1955 , p. 461,464
Journal of the Chemical Society, 1959 , p. 1027,1030
