3-甲基-CBS-氧硼啶合成路线 （共 731 条）
参考文献
Journal of Organic Chemistry, , vol. 56, # 18 p. 751 - 762
反应条件
1: in tetrahydrofuran T=0°C; Grignard reaction; 3.5 h; Inert atmosphere; 2: With potassium hydroxide in methanol 24 h; Reflux;
参考文献
Chemistry - A European Journal, , vol. 16, # 1 p. 95 - 99
反应条件
1: diethyl ether 2: (i) HC(OEt)3, (ii) (heating) View Scheme
参考文献
Kopecky,K.R. et al.
Canadian Journal of Chemistry, 1978 , vol. 56, p. 1114 - 1121
反应条件
1: diethyl ether; benzene / 20 °C 3: palladium/charcoal / 280 - 320 °C 4: concentrated aqueous HBr; glacial acetic acid View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
反应条件
formic acid ethyl ester 1.) ether, 2 h, 2.) ether, 2 h; Yield given. Multistep reaction;
参考文献
Lapkin, I. I.; Kolbina, N. M.; Tatarenko, O. I.; Prokhorova, T. S.; Gartman, G. A.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 11 p. 778 - 779
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 11 p. 1326 - 1328
反应条件
1.) ether,heating,2h, 2.) heating,2h; Yield given. Multistep reaction;
参考文献
Lapkin, I. I.; Kolbina, N. M.; Tatarenko, O. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 2 p. 279 - 281
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 315 - 317
参考文献
Gilbert, Jacques; Fuentes, Maryse; Ojasoo, Tiiu; Dore, Jean-Christophe; Pons, Michel
Journal of Medicinal Chemistry, 1997 , vol. 40, # 7 p. 1104 - 1111
反应条件
samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=25°C; 0.5 h;
参考文献
Fukuzawa, Shin-Ichi; Furuya, Hideki; Tsuchimoto, Teruhisa
Tetrahedron, 1996 , vol. 52, # 6 p. 1953 - 1960
反应条件
ethylmagnesium bromide; iron(III) chloride
参考文献
Bietti, Massimo; Capone, Alberto
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 618 - 629
反应条件
CoCl2 in tetrahydrofuran; diethyl ether T=-40°C; 24 h;
参考文献
Korn, Tobias J.; Schade, Matthias A.; Cheemala, Murthy N.; Wirth, Stefan; Guevara, Simon A.; Cahiez, Gerard; Knochel, Paul
Synthesis, 2006 , # 21 p. 3547 - 3574
