3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
copper(l) iodide; boron trifluoride diethyl etherate in tetrahydrofuran T=-30 - 0°C; 1 h;
参考文献
Hayes, Jerome F.; Shipman, Michael; Twin, Heather
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 935 - 942
参考文献
Quelet; Golse
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 159
Full Text Show Details
Marvel; Hein
Journal of the American Chemical Society, 1948 , vol. 70, p. 1895,1897
反应条件
1: chlorobenzene With HASPO; Ni(acac)2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: 4-methoxyphenyl magnesium bromide in tetrahydrofuran T=20°C; Kumada cross-coupling; 4 h;
参考文献
Liu, Ning; Wang, Zhong-Xia
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10031 - 10038
反应条件
C35H31BrN4NiP in tetrahydrofuran T=25°C; 17 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
PinP(O)H; [Pd(dibenzylideneacetone)2] in tetrahydrofuran; 1,4-dioxane T=80°C; Kumada cross-coupling reaction; 22 h;
参考文献
Ackermann, Lutz; Althammer, Andreas
Organic Letters, 2006 , vol. 8, # 16 p. 3457 - 3460
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 24 h; Heating;
参考文献
Shirakawa, Eiji; Okura, Keisho; Uchiyama, Nanase; Murakami, Takuya; Hayashi, Tamio
Chemistry Letters, 2014 , vol. 43, # 6 p. 922 - 924
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2010 , vol. 12, # 19 p. 4388 - 4391
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=20°C; 21 h;
参考文献
Organic Letters, , vol. 7, # 7 p. 1219 - 1222
反应条件
Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran T=50°C; Kumada-Corriu reaction; 24 h;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
