3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
C68H72Cl2N6NiP2 in diethyl ether T=25°C; Kumada coupling reaction; 12 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
反应条件
C80H88Cl2N6NiP2 in diethyl ether T=25°C; Kumada coupling reaction; 12 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 48 h; Inert atmosphere;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2010 , vol. 12, # 19 p. 4388 - 4391
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 48 h; Inert atmosphere;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2010 , vol. 12, # 19 p. 4388 - 4391
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; 48 h; Inert atmosphere;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2010 , vol. 12, # 19 p. 4388 - 4391
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 91 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Cella, Rodrigo; Cunha, Rodrigo L. O. R.; Reis, Ana E. S.; Pimenta, Daniel C.; Klitzke, Clecio F.; Stefani, Helio A.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 244 - 250
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran T=20°C; 5 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Uemura, Sakae; Fukuzawa, Shin-ichi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1181 - 1184
反应条件
methanesulfonic acid,phenyl ester; zinc; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran 10 h; Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 6895 - 6903
反应条件
zinc; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran 10 h; Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 6895 - 6903
反应条件
bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride in tetrahydrofuran; diethyl ether T=20°C; 0.0833333 h; absence of ZnCl2, oth. Pd catalyst, oth. time; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 7 p. 1222 - 1231
Zhurnal Organicheskoi Khimii, , vol. 23, # 7 p. 1354 - 1364
