3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: 1,3-dichloro-2-iodobenzene; 4-methoxyphenyl magnesium bromide 2: With iodine
参考文献
Wright, Ryan S.; Vinod, Thottumkara K.
Tetrahedron Letters, 2003 , vol. 44, # 38 p. 7129 - 7132
反应条件
palladium diacetate in tetrahydrofuran for 2 h at -20°C;
参考文献
Yasuda, Shigeo; Yorimitsu, Hideki; Oshima, Koichiro
Organometallics, 2008 , vol. 27, # 16 p. 4025 - 4027
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Konno, Tsutomu; Takehana, Tsuyoshi; Mishima, Makoto; Ishihara, Takashi
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3545 - 3550
反应条件
in tetrahydrofuran 0.5 h;
参考文献
Meyers; Sun; Carlson; Marriner; Katzenellenbogen
Journal of Medicinal Chemistry, 2001 , vol. 44, # 24 p. 4230 - 4251
反应条件
1: 4-methoxyphenyl magnesium bromide With (DABCO)*(SO2)2 in tetrahydrofuran T=-40°C; 1 h; Inert atmosphere; 2: Diphenyliodonium triflate in N,N-dimethyl-formamide T=120°C; 5 h; Inert atmosphereMicrowave irradiation;
参考文献
Deeming, Alex S.; Russell, Claire J.; Hennessy, Alan J.; Willis, Michael C.
Organic Letters, 2014 , vol. 16, # 1 p. 150 - 153
反应条件
1: anfangs in Aether, zuletzt in Benzol oder Toluol bei Siedetemperatur 2: diethyl ether; SOCl2 / zuletzt Behandeln bei Siedetemperatur View Scheme
参考文献
Hardegger; Redlich; Gal
Helvetica Chimica Acta, 1945 , vol. 28, p. 628,633
反应条件
copper(l) iodide in tetrahydrofuran T=70°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
1: diethyl ether 2: potassium hydrogen sulfate / 160 °C / 10 Torr 3: Raney nickel; methanol / Hydrogenation.Erhitzen des Reaktionsprodukts mit Essigsaeure und wss. Bromwasserstoffsaeure View Scheme
参考文献
Ziering et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 894,897, 9O2
反应条件
N,N,N',N,-tetramethylethylenediamine; Co(acac)3 in tetrahydrofuran T=0°C; 0.666667 h; Inert atmosphere; chemoselective reaction;
参考文献
Cahiez, Gerard; Chaboche, Christophe; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2009 , vol. 11, # 2 p. 277 - 280
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=80°C; 2 h;
参考文献
Rao Volla, Chandra M.; Vogel, Pierre
Angewandte Chemie - International Edition, 2008 , vol. 47, # 7 p. 1305 - 1307
