3-甲基-CBS-氧硼啶合成路线 (共 731 条)
参考文献
McKenzie; Pirie
Chemische Berichte, 1936 , vol. 69, p. 861,875
反应条件
in tetrahydrofuran Grignard reaction;
参考文献
Mukaiyama, Teruaki; Yanagisawa, Manabu; Iida, Daisuke; Hachiya, Iwao
Chemistry Letters, 2000 , # 6 p. 606 - 607
参考文献
Weizmann; Bergmann; Bergmann
Journal of the Chemical Society, 1935 , p. 1367,1368, 1369
反应条件
1: benzene; diethyl ether 2: benzene View Scheme
参考文献
Marvel; Whitson; Johnston
Journal of the American Chemical Society, 1944 , vol. 66, p. 415
反应条件
1-methyl-pyrrolidin-2-one; copper dichloride in tetrahydrofuran T=0°C; 1.3 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 7 p. 1278 - 1281
反应条件
in diethyl ether T=-78°C;
参考文献
Journal of Organic Chemistry, , vol. 45, # 13 p. 2727 - 2729
反应条件
diisobutylaluminium hydride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 16 h; Ambient temperaturefurther temperature and reaction time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 27, # 49 p. 6013 - 6016
反应条件
1: in tetrahydrofuran T=-20°C; 1 h; 2: With sodium tetrahydroborate; iron(II) chloride in tetrahydrofuran; ethanol T=20°C; 2 h;
参考文献
Kopp, Felix; Sapountzis, Ioannis; Knochel, Paul
Synlett, 2003 , # 6 p. 885 - 887
反应条件
Co(acetylacetonate)3; 2-chlorostyrene in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=30°C; 0.333333 h;
参考文献
Guelak, Samet; Stepanek, Ondrej; Malberg, Jennifer; Rad, Babak Rezaei; Kotora, Martin; Wolf, Robert; Jacobi Von Wangelin, Axel
Chemical Science, 2013 , vol. 4, # 2 p. 776 - 784
反应条件
3: peroxyformic acid; KMnO4 View Scheme
参考文献
Pascual; Crespo
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1952 , vol. <B> 48, p. 273,276