3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
hydrogenchloride 1.) THF, RT, overnight, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Gupton, John T.; Norman, Bryan; Wysong, Ernest
Synthetic Communications, 1985 , vol. 15, # 14 p. 1305 - 1314
参考文献
Jutz
Chemische Berichte, 1958 , vol. 91, p. 1867,1876
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Garst, Michael E.; Lukton, David
Synthetic Communications, 1980 , vol. 10, # 2 p. 155 - 160
反应条件
1: With copper(l) iodide; trimethylsilyl trifluoromethanesulfonate; lithium chloride in tetrahydrofuran T=-78°C; 1 h; 2: With trifluoroacetic acid in tetrahydrofuran T=-78 - 20°C; Further stages.;
参考文献
Mueller, Amanda J.; Jennings, Michael P.
Organic Letters, 2007 , vol. 9, # 25 p. 5327 - 5329
反应条件
hydrogenchloride 1.) THF, RT, overnight, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Gupton, John T.; Norman, Bryan; Wysong, Ernest
Synthetic Communications, 1985 , vol. 15, # 14 p. 1305 - 1314
参考文献
Jutz
Chemische Berichte, 1958 , vol. 91, p. 1867,1876
参考文献
Hickinbottom; Rogers
Journal of the Chemical Society, 1957 , p. 4124,4129
反应条件
1: 4-methoxyphenyl magnesium bromide With titanium(IV) isopropylate in tetrahydrofuran; toluene T=-40°C; 0.0833333 h; Inert atmosphere; 2: N-chloro-morpholine in tetrahydrofuran; toluene T=-40 - 20°C; 4 h; Inert atmosphere;
参考文献
Barker, Timothy J.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8325 - 8328
反应条件
in dichloromethane T=-78°C;
参考文献
Ruano, Jose L. Garcia; Alemparte, Carlos; Aranda, M. Teresa; Zarzuelo, Maria M.
Organic Letters, 2003 , vol. 5, # 1 p. 75 - 78
反应条件
in dichloromethane T=-78°C;
参考文献
Ruano, Jose L. Garcia; Alemparte, Carlos; Aranda, M. Teresa; Zarzuelo, Maria M.
Organic Letters, 2003 , vol. 5, # 1 p. 75 - 78
