3-甲基-CBS-氧硼啶合成路线 （共 731 条）
参考文献
Grignard; Zorn
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 150, p. 1179
反应条件
copper(I) bromide; lithium bromide in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere;
参考文献
Jiang, Xiaolu; London, Emma K.; Morris, David J.; Clarkson, Guy J.; Wills, Martin
Tetrahedron, 2010 , vol. 66, # 52 p. 9828 - 9834
反应条件
1: diethyl ether; benzene 2: pyridine; SOCl2 View Scheme
参考文献
Bhattacharyya
Journal of the Indian Chemical Society, 1945 , vol. 22, p. 165,167
参考文献
Sulzbacher
Journal of Applied Chemistry, 1951 , vol. 1, p. 95
参考文献
Bordwell; Boutan
Journal of the American Chemical Society, 1957 , vol. 79, p. 717,722
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Bordwell; Pitt
Journal of the American Chemical Society, 1955 , vol. 77, p. 572,576
反应条件
1: in tetrahydrofuran T=0 - 60°C; 7.17 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=0 - 20°C;
参考文献
GLAXO GROUP LIMITED; TEMPERO PHARMACEUTICALS, INC.; BALOGLU, Erkan; GHOSH, Shomir; LOBERA, Mercedes; SCHMIDT, Darby; WANG, Yonghui
Patent: WO2013/85890 A1, 2013 ;
Location in patent: Page/Page column 33 ;
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 76 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Denmark, Scott E.; Wu, Zhicai
Organic Letters, 1999 , vol. 1, # 9 p. 1495 - 1498
反应条件
diethyl ether; toluene
参考文献
Gilman; Beaber; Myers
Journal of the American Chemical Society, 1925 , vol. 47, p. 2050
反应条件
diethyl ether; trichlorophosphate
参考文献
Kosolapoff
Journal of the American Chemical Society, 1949 , vol. 71, p. 369
反应条件
diethyl ether und anschliessenden Behandeln mit wss.Salzsaeure;
参考文献
Kosolapoff
Journal of the American Chemical Society, 1949 , vol. 71, p. 369
