3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
diethyl ether; benzene
参考文献
Geyer
Journal of the American Chemical Society, 1942 , vol. 64, p. 2226
反应条件
1: diethyl ether 2: potassium hydrogen sulfate / 160 °C / 10 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 12, p. 894,897, 9O2
反应条件
1: 1-chloro-4-isopropenylbenzene With [Co(PPh3)3Cl] 2: 4-methoxyphenyl magnesium bromide 0.333333 h;
参考文献
Guelak, Samet; Stepanek, Ondrej; Malberg, Jennifer; Rad, Babak Rezaei; Kotora, Martin; Wolf, Robert; Jacobi Von Wangelin, Axel
Chemical Science, 2013 , vol. 4, # 2 p. 776 - 784
反应条件
1: 1-chloro-2-(isopropenyl)benzene With [Co(PPh3)3Cl] 2: 4-methoxyphenyl magnesium bromide 0.333333 h;
参考文献
Guelak, Samet; Stepanek, Ondrej; Malberg, Jennifer; Rad, Babak Rezaei; Kotora, Martin; Wolf, Robert; Jacobi Von Wangelin, Axel
Chemical Science, 2013 , vol. 4, # 2 p. 776 - 784
反应条件
in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Koo, Ja Seo; Lee, Jae In
Synthetic Communications, 1996 , vol. 26, # 20 p. 3709 - 3713
参考文献
Grignard; Bellet; Courtot
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 47
反应条件
anhydrous iron chloride; 1,2-dichloro-ethane in tetrahydrofuran T=0°C; 0.0833333 h; Ionic liquidInert atmosphere;
参考文献
Kude, Keisuke; Hayase, Shuichi; Kawatsura, Motoi; Itoh, Toshiyuki
Heteroatom Chemistry, 2011 , vol. 22, # 3-4 p. 397 - 404
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; 6 h;
参考文献
Helbig, Sarah; Axenov, Kirill V.; Tussetschlaeger, Stefan; Frey, Wolfgang; Laschat, Sabine
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3506 - 3509
反应条件
1: 1-bromocyclohexane With [Fe(C2H4)4][Li(tmeda)]2 in tetrahydrofuran T=-20°C; 2: 4-methoxyphenyl magnesium bromide in tetrahydrofuran; diethyl ether T=-20°C; Further stages.;
参考文献
Fuerstner, Alois; Martin, Ruben; Krause, Helga; Seidel, Guenter; Goddard, Richard; Lehmann, Christian W.
Journal of the American Chemical Society, 2008 , vol. 130, # 27 p. 8773 - 8787
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 19 art. no. SS-2013-T0413-OP, p. 2752 - 2762
