3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
FeCl(THF)L1 in diethyl ether T=20°C; 0.5 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
UNIVERSITY OF PRINCE EDWARD ISLAND; GENESIS GROUP INC.; SHAVER, Michael, P.; KOZAK, Christopher, M.
Patent: WO2013/53046 A1, 2013 ;
Location in patent: Paragraph 00282-00284 ;
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran T=20°C; 5 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Uemura, Sakae; Fukuzawa, Shin-ichi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1181 - 1184
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
methanesulfonic acid,phenyl ester; zinc; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran 10 h; Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 6895 - 6903
反应条件
[Pt(PPh3)4] in hexane T=55°C; 10 h; stereoselective reaction;
参考文献
Yang, Dingqiao; Liang, Ni
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 13 p. 2080 - 2086
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 18 h; Heating;
参考文献
Tetrahedron, , vol. 63, # 20 p. 4304 - 4309
反应条件
copper(I) bromide in tetrahydrofuran 1 h; ice-bath;
参考文献
McDonald, Edward; Smith, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 837 - 842
