3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: With nickel dichloride T=20°C; Kumada-Tamao-Corriu cross-coupling; 3 h; 2: With water; ammonium chloride
参考文献
Shibahara, Fumitoshi; Yamaguchi, Eiji; Kitagawa, Asumi; Imai, Akio; Murai, Toshiaki
Tetrahedron, 2009 , vol. 65, # 26 p. 5062 - 5073
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=-78°C; 1 h;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 1012 - 1014
反应条件
diisobutylaluminium hydride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 16 h; Ambient temperaturefurther temperature and reaction time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 27, # 49 p. 6013 - 6016
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
参考文献
Takahashi, Hidetaka; Ohe, Kouichi; Uemura, Sakae; Sugita, Nobuyuki
Journal of Organometallic Chemistry, 1988 , vol. 350, p. 227 - 234
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether T=20°C; 0.25 h; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1696 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1858 - 1865
反应条件
diisobutylaluminium hydride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 16 h; Ambient temperaturefurther temperature and reaction time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 27, # 49 p. 6013 - 6016
反应条件
copper(l) iodide in tetrahydrofuran 48 h; Ambient temperature; Yield given;
参考文献
Buergi, Christoph; Liu, Gui; Rueedi, Peter
Helvetica Chimica Acta, 1993 , vol. 76, p. 1901 - 1915
反应条件
copper(I) bromide in tetrahydrofuran 1 h;
参考文献
McDonald, Edward; Smith, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 837 - 842
反应条件
copper(l) iodide 1.) THF, ether, -78 deg C, 2.) THF, ether, from -78 deg C to RT; Yield given. Multistep reaction;
参考文献
Kume, Takashi; Kojima, Toshikatsu; Iwasaki, Hideharu; Yamamoto, Yohsuke; Akiba, Kin-ya
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1931 - 1935
反应条件
boron trifluoride diethyl etherate 1.)ethyl trimethylsilylacetate, ether, -78 grad C, warmed to rt., stirred overnight, 2.) BF3OEt2, CH2Cl2, 2 h, rt.; Yield given. Multistep reaction;
参考文献
Larson, Gerald L.; Hernandez, David
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1035 - 1038
