3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 10 p. 780 - 781
反应条件
in diethyl ether T=25°C; 1 h;
参考文献
Golovchenko, L. S.; Pombrik, S. I.; Peregudov, A. S.; Kravtsov, D. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 3 p. 610 - 613
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 3 p. 668 - 672
反应条件
silver nitrate in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Murakami, Kei; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2008 , vol. 47, # 31 p. 5833 - 5835
反应条件
1: p-toluidine With n-butyllithium; ZnCl2*TMEDA in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; Inert atmosphereSchlenk technique; 2: 4-methoxyphenyl magnesium bromide With N,N'-dimethyl-N,N'-propyleneurea; bis(acetylacetonate)nickel(II); 1,2-dichloro-2-methylpropane in tetrahydrofuran; hexane T=0 - 20°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Ilies, Laurean; Matsubara, Tatsuaki; Nakamura, Eiichi
Organic Letters, 2012 , vol. 14, # 21 p. 5570 - 5573,4
反应条件
in tetrahydrofuran T=-15 - 20°C; 1.5 h;
参考文献
Lee, Jae In
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 3 p. 749 - 752
反应条件
diethyl ether; tellurium(II) bromide
参考文献
Lederer
Chemische Berichte, 1920 , vol. 53, p. 713
反应条件
in toluene T=0 - 20°C;
参考文献
Hawkins, Vanessa F.; Wilkinson, Mark C.; Whiting, Matthew
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1265 - 1268
反应条件
in tetrahydrofuran T=25°C; 1 h; Inert atmosphere;
参考文献
Clary, Jacob W.; Rettenmaier, Terry J.; Snelling, Rachel; Bryks, Whitney; Banwell, Jesse; Wipke, W. Todd; Singaram, Bakthan
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9602 - 9610
反应条件
1: in toluene T=0 - 20°C; 2: in toluene T=50°C;
参考文献
Hawkins, Vanessa F.; Wilkinson, Mark C.; Whiting, Matthew
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1265 - 1268
反应条件
1: 4-methoxyphenyl magnesium bromide With diethylaluminium chloride in tetrahydrofuran; hexane T=0 - 20°C; 3 h; Schlenk technique; 2: 4-methoxy-1-vinyl-benzene With [RhCl(η2:η2-cycloocta-1,5-diene)]2; 2,4-dimethylpentan-3-one T=60°C; 3 h;
参考文献
Tanaka, Shota; Mori, Atsunori
European Journal of Organic Chemistry, 2014 , vol. 2014, # 6 p. 1167 - 1171
