3-甲基-CBS-氧硼啶合成路线 （共 731 条）
参考文献
Lawesson; Yang
Journal of the American Chemical Society, 1959 , vol. 81, p. 4230,4232
反应条件
hydrogenchloride
1.) THF, 66 deg C, 2 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rahman, M. T.; Nur, H. P.
Journal of the Indian Chemical Society, 1994 , vol. 71, # 6-8 p. 469 - 474
反应条件
anhydrous iron chloride in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Kozak, Christopher M.
Synlett, 2011 , # 6 p. 852 - 856
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=80°C; 2 h;
参考文献
Rao Volla, Chandra M.; Vogel, Pierre
Angewandte Chemie - International Edition, 2008 , vol. 47, # 7 p. 1305 - 1307
反应条件
1: (i), (ii) TsOH
2: H2 / Raney-Ni
View Scheme
参考文献
Zavgorodnii,S.V.; Kozlikovskii,Y.B.
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 4 p. 799 - 803,809 - 812
反应条件
N,N,N',N,-tetramethylethylenediamine; ((Me)N2N)Ni-Cl in tetrahydrofuran
T=20°C; Kumada-Corriu-Tamao coupling reaction; 2 h; Inert atmosphere;
参考文献
Vechorkin, Oleg; Proust, Valerie; Hu, Xile
Journal of the American Chemical Society, 2009 , vol. 131, # 28 p. 9756 - 9766
反应条件
N,N,N',N,-tetramethylethylenediamine; ((Me)N2N)Ni-Cl in tetrahydrofuran
T=20°C; Kumada-Corriu-Tamao coupling reaction; 2 h; Inert atmosphere;
参考文献
Vechorkin, Oleg; Proust, Valerie; Hu, Xile
Journal of the American Chemical Society, 2009 , vol. 131, # 28 p. 9756 - 9766
反应条件
anhydrous iron chloride; Ipr.HCl in tetrahydrofuran
T=0 - 40°C; 1.66667 h;
参考文献
Ghorai, Sujit K.; Jin, Masayoshi; Hatakeyama, Takuji; Nakamura, Masaharu
Organic Letters, 2012 , vol. 14, # 4 p. 1066 - 1069
反应条件
copper(l) iodide in tetrahydrofuran
T=70°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
diethyl ether
Behandeln des Reaktionsprodukts mit Aethanol und Natrium;
参考文献
Normant
Annales de Chimie (Cachan, France), 1942 , vol. <11> 17, p. 335,346
