3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Knapp, Kolja M.; Goldfuss, Bernd; Knochel, Paul
Chemistry - A European Journal, 2003 , vol. 9, # 21 p. 5259 - 5265
反应条件
1: silicon tetrachloride / diethyl ether / -20 - 20 °C
2: 7.5 g / diethyl ether / 12 h / Heating
View Scheme
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
trichlorosilane in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Knoelker, Hans-Joachim; Foitzik, Norbert; Goesmann, Helmut; Graf, Regina; Jones, Peter G.; Wanzl, Guenter
Chemistry - A European Journal, 1997 , vol. 3, # 4 p. 538 - 551
参考文献
Gmelin Handbook: Si: MVol.C, 36, page 111 - 115
反应条件
1: Cp2Sm / tetrahydrofuran / a) -78 deg C, 15 min, b) RT, 1 h
2: pyridine / Ambient temperature
View Scheme
参考文献
Fukuzawa, Shin-Ichi; Furuya, Hideki; Tsuchimoto, Teruhisa
Tetrahedron, 1996 , vol. 52, # 6 p. 1953 - 1960
反应条件
CoCl2 in tetrahydrofuran; diethyl ether
T=-40°C; 24 h;
参考文献
Korn, Tobias J.; Schade, Matthias A.; Cheemala, Murthy N.; Wirth, Stefan; Guevara, Simon A.; Cahiez, Gerard; Knochel, Paul
Synthesis, 2006 , # 21 p. 3547 - 3574
反应条件
tetrachlorosilane in diethyl ether
T=-20 - 20°C;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
参考文献
Gmelin Handbook: Si: MVol.C, 57, page 162 - 165
反应条件
in tetrahydrofuran
T=23 - 60°C;
参考文献
PRESIDENT AND FELLOWS OF HARVARD COLLEGE; RITTER, Tobias; FURUYA, Takeru; TANG, Pingping
Patent: WO2010/59943 A2, 2010 ;
Location in patent: Page/Page column 46 ;
反应条件
in tetrahydrofuran
Bu3SnCl and Grignard reagent in THF; distn. under reduced pressure;
参考文献
Uemura; Ohe; Motofusa
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 7 p. 1343 - 1348
