3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in toluene
T=60°C; 4 h;
参考文献
Itami, Kenichiro; Yamazaki, Daisuke; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 47 p. 15396 - 15397
反应条件
in tetrahydrofuran
T=-42 - 20°C;
参考文献
Kakiya, Hirotada; Yagi, Kazunari; Shinokubo, Hiroshi; Oshima, Koichiro
Journal of the American Chemical Society, 2002 , vol. 124, # 31 p. 9032 - 9033
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
1.) ether, reflux, 3 h, 2.) CH2Cl2, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Luis; Fletcher; Echeverri; Grillo
Tetrahedron, 1994 , vol. 50, # 37 p. 10963 - 10970
参考文献
Welsh; Drake
Journal of the American Chemical Society, 1938 , vol. 60, p. 59,61
参考文献
Peck
Journal of the American Chemical Society, 1956 , vol. 78, p. 997,1000
反应条件
in tetrahydrofuran
T=20°C; 1 h;
参考文献
Li, Guijie; Zhou, Shaolin; Su, Guowei; Liu, Yuanhong; Wang, Peng George
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9830 - 9833
反应条件
2: 85 percent / pyridine hydrochloride / 0.75 h / 200 - 220 °C
View Scheme
参考文献
Gilbert, Jacques; Fuentes, Maryse; Ojasoo, Tiiu; Dore, Jean-Christophe; Pons, Michel
Journal of Medicinal Chemistry, 1997 , vol. 40, # 7 p. 1104 - 1111
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
Lloyd, John R.; Lowther, Nicholas; Hall, C. Dennis
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 245 - 250
反应条件
1: diethyl ether
2: aqueous H2SO4; ethanol
View Scheme
参考文献
Kenyon; Mason
Journal of the Chemical Society, 1952 , p. 4964,4966
反应条件
iron (III) acetylacetonate in tetrahydrofuran
T=-30 - -20°C; 3 h;
参考文献
Quintin, Jerome; Roullier, Catherine; Thoret, Sylviane; Lewin, Guy
Tetrahedron, 2006 , vol. 62, # 17 p. 4038 - 4051
