3-甲基-CBS-氧硼啶合成路线 （共 731 条）
参考文献
Hilbert; Johnson
Journal of the American Chemical Society, 1929 , vol. 51, p. 1533
反应条件
1.1: 69 percent / benzene / Heating
2.1: Na / diethyl ether / Heating
2.2: 2.3 percent / acetonitrile / 20 °C
View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
反应条件
in tetrahydrofuran
-78 deg C, 30 min; r.t., 1 h;
参考文献
Chikashita, Hidenori; Komazawa, Shun-ichiro; Ishimoto, Nishiki; Inoue, Koji; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1215 - 1225
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(I) bromide in tetrahydrofuran
Reflux;
参考文献
Shimizu, Tomoe; Kato, Rika; Miyamoto, Shinpei; Yamato, Takehiko
Journal of Chemical Research, 2010 , # 8 p. 445 - 448
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
anhydrous iron chloride in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Kozak, Christopher M.
Synlett, 2011 , # 6 p. 852 - 856
反应条件
1: diethyl ether; benzene
2: N.N-dimethyl-aniline; SOCl2
3: diethyl ether; magnesium
View Scheme
参考文献
Bhattacharyya
Journal of the Indian Chemical Society, 1945 , vol. 22, p. 165,167
参考文献
Bolton, Roger; Mguni, Raphael S.; Williams, Gareth H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 405 - 408
参考文献
Toone,T.W. et al.
Canadian Journal of Chemistry, 1975 , vol. 53, p. 1635 - 1641
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether
5 h; Ambient temperature;
参考文献
He, Zhen-Min; Rice, Joseph E.; LaVoie, Edmond J.
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1784 - 1789
