3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
in tetrahydrofuran; toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Hayashi, Yumi; Itoh, Ken-Ichi; Watabe, Ryo; Uchiyama, Nanase; Konagaya, Wataru; Masui, Seiji; Hayashi, Tamio
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 218 - 221
反应条件
Ni(PCy3)2Cl2 in toluene
T=30°C; Kumada-Tamao-Corriu coupling; 1 h; Inert atmosphere;
参考文献
Zhao, Fei; Yu, Da-Gang; Zhu, Ru-Yi; Xi, Zhenfeng; Shi, Zhang-Jie
Chemistry Letters, 2011 , vol. 40, # 9 p. 1001 - 1003
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran
48 h; Heating;
参考文献
Cho, Chul-Hee; Park, Heon; Park, Min-Ah; Ryoo, Tae-Yong; Lee, Yoon-Sik; Park, Kwangyong
European Journal of Organic Chemistry, 2005 , # 15 p. 3177 - 3181
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=30°C; 2 h; Inert atmosphere;
参考文献
Guelak, Samet; Jacobivonwangelin, Axel
Angewandte Chemie - International Edition, 2012 , vol. 51, # 6 p. 1357 - 1361
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
3 h; Heating;
参考文献
Mewshaw, Richard E.; Edsall Jr., Richard J.; Yang, Cuijian; Manas, Eric S.; Xu, Zhang B.; Henderson, Ruth A.; Keith Jr., James C.; Harris, Heather A.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 12 p. 3953 - 3979
参考文献
Bachmann
Journal of the American Chemical Society, 1932 , vol. 54, p. 1969,1970
Journal of the American Chemical Society, 1933 , vol. 55, p. 1179,1186
反应条件
[1,3-bis(2,6-diisopropylphenyl)-imidazolium][Ni(PPh3)Cl3] in tetrahydrofuran
T=30°C; Kumada Cross-Coupling; 5 h; Schlenk techniqueInert atmosphere;
参考文献
Xu, Yan-Chao; Zhang, Jie; Sun, Hong-Mei; Shen, Qi; Zhang, Yong
Dalton Transactions, 2013 , vol. 42, # 23 p. 8437 - 8445
反应条件
C35H31BrN4NiP in tetrahydrofuran
T=25°C; 11 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
PinP(O)H; [Pd(dibenzylideneacetone)2] in tetrahydrofuran; 1,4-dioxane
T=80°C; Kumada cross-coupling reaction; 22 h;
参考文献
Ackermann, Lutz; Althammer, Andreas
Organic Letters, 2006 , vol. 8, # 16 p. 3457 - 3460
反应条件
bis(acetylacetonate)nickel(II); 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran
T=20°C; Corriu-Kumada-Tamao coupling; 18 h;
参考文献
Parmentier, Michael; Gros, Philippe; Fort, Yves
Tetrahedron, 2005 , vol. 61, # 13 p. 3261 - 3269
