3-甲基-CBS-氧硼啶合成路线 (共 731 条)
参考文献
Holmberg
Acta Academiae Aboensis, Series B: Mathematica et Physica, 1949 , vol. 16, # 6 p. 72
Chem.Abstr., 1951 , p. 558
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran T=20°C; Kumada-Corriu-Tamao coupling reaction;
参考文献
Leblond, Jeanne; Gao, Hui; Petitjean, Anne; Leroux, Jean-Christophe
Journal of the American Chemical Society, 2010 , vol. 132, # 25 p. 8544 - 8545
反应条件
N,N,N',N,-tetramethylethylenediamine; Co(acac)3 in tetrahydrofuran T=0°C; 0.666667 h; Inert atmosphere; chemoselective reaction;
参考文献
Cahiez, Gerard; Chaboche, Christophe; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2009 , vol. 11, # 2 p. 277 - 280
反应条件
2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Dewar; Puttnam
Journal of the Chemical Society, 1959 , p. 4080,4084
参考文献
Hickinbottom; Rogers
Journal of the Chemical Society, 1957 , p. 4124,4129
反应条件
1: 82 percent / diethyl ether 2: 96 percent / H2 / 10percent Pd/C / ethanol / 48 h / 25 °C / 3105.2 Torr View Scheme
参考文献
Collins, David J.; Jacobs, Howard A.
Australian Journal of Chemistry, 1987 , vol. 40, # 12 p. 1989 - 2004
反应条件
iron(III) chloride amine-bis(phenolate) complex in diethyl ether; dichloromethane 0.5 h;
参考文献
Chowdhury, Rajoshree Roy; Crane, Angela K.; Fowler, Candace; Kwong, Philip; Kozak, Christopher M.
Chemical Communications, 2008 , # 1 p. 94 - 96
参考文献
Golubev, Oleg; Panov, Dmitri; Ploom, Anu; Tuulmets, Ants; Nguyen, Binh T.
Journal of Organometallic Chemistry, 2007 , vol. 692, # 17 p. 3700 - 3705
反应条件
((C6H4)(PPh2)(NCHPhP(O)Ph2))NiCl in tetrahydrofuran T=70°C; Kumada cross-coupling; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Zhong-Xia
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10031 - 10038
反应条件
1: 2.) bromine 2: thionyl chloride / 2 h / Heating View Scheme
参考文献
Harger, Martin J. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3284 - 3288