3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: in tetrahydrofuran
T=-40 - 0°C; 1 h;
2: With trifluoroacetic acid in tetrahydrofuran
T=25°C; 1.5 h;
参考文献
Hamura, Toshiyuki; Nakayama, Ryosuke
Chemistry Letters, 2013 , vol. 42, # 9 p. 1013 - 1015
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Benderradji, Farah; Nechab, Malek; Einhorn, Cathy; Einhorn, Jacques
Synlett, 2006 , # 13 p. 2035 - 2038
反应条件
diethyl ether; benzene
Erwaermen des Reaktionsprodukts in Aceton mit wss. Salzsaeure;
参考文献
Blicke; Patelski
Journal of the American Chemical Society, 1936 , vol. 58, p. 559,561
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=-40°C; 3 h; chemoselective reaction;
参考文献
Hatakeyama, Takuji; Yoshimoto, Yuya; Ghorai, Sujit K.; Nakamura, Masaharu
Organic Letters, 2010 , vol. 12, # 7 p. 1516 - 1519
反应条件
1: 89 percent / Pd[P(Ph)3]4 / tetrahydrofuran / 3 h / Heating
2: 89 percent / C6H5N*HCl / 2 h / 190 °C
View Scheme
参考文献
Mewshaw, Richard E.; Edsall Jr., Richard J.; Yang, Cuijian; Manas, Eric S.; Xu, Zhang B.; Henderson, Ruth A.; Keith Jr., James C.; Harris, Heather A.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 12 p. 3953 - 3979
反应条件
N-chloro-succinimide; triethylamine
1.) ether; Yield given. Multistep reaction;
参考文献
Konno, Shoetsu; Sagi, Mataichi; Yoshida, Nobuko; Yamanaka, Hiroshi
Heterocycles, 1987 , vol. 26, # 12 p. 3111 - 3114
反应条件
in tetrahydrofuran
addn. of a soln. of SnCl4 to a soln. of organic compound under cooling, heating for 12 h under reflux; addn. of HCl, reccrystn., elem. anal.;
参考文献
Schneider-Koglin, Claudia; Mathiasch, Bernd; Draeger, Martin
Journal of Organometallic Chemistry, 1994 , vol. 469, # 1 p. 25 - 32
反应条件
(i) CrCl3, THF, (ii) /BRN= 1361340/; Multistep reaction;
参考文献
Sneeden,R.P.A.; Zeiss,H.H.
Journal of Organometallic Chemistry, 1972 , vol. 40, p. 163 - 174
参考文献
Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 187, p. 662
反应条件
in diethyl ether
Grignard reaction; ice-bath temperature;
参考文献
Fujio, Mizue; Morimoto, Hiroshi; Kim, Hyun-Joong; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 6 p. 1403 - 1411
