反应条件
1: thionyl chloride / CCl4
2: CH2Cl2 / a) 40 deg C, 3 h, b) RT, 15 h
3: 80 percent / Zn, AcOH / H2O / 0.08 h / Ambient temperature
View Scheme
参考文献
Chollet; Miginiac; Rudelle; Bonnemain
Synthetic Communications, 1993 , vol. 23, # 15 p. 2101 - 2111