[(叔丁氧羰基氨基)甲基]三氟硼酸钾合成路线 （共 25 条）
反应条件
1.1: potassium hexamethylsilazane / tetrahydrofuran / 2.25 h / -78 - 20 °C 1.2: 1 h / 0 °C 1.3: 0 - 20 °C 2.1: KHF2 / methanol; water / 0 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 13, # 15 p. 3956 - 3959
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in water; toluene T=85°C; Suzuki-Miyaura cross-coupling reaction; 22 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2011 , vol. 13, # 15 p. 3956 - 3959
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; dichloro(cycloocta-1,5-diene)palladium(II) in water; tert-butyl alcohol T=95°C; Suzuki-Miyaura cross-coupling; 22 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2012 , vol. 14, # 12 p. 3138 - 3141
反应条件
palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; toluene T=85°C; Suzuki-Miyaura cross-coupling reaction; 22 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2011 , vol. 13, # 15 p. 3956 - 3959
反应条件
C45H59ClNPPd; potassium carbonate in water; tert-butyl alcohol T=85°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2013 , vol. 15, # 10 p. 2534 - 2537
反应条件
C45H59ClNPPd; potassium carbonate in water; tert-butyl alcohol T=85°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 10 p. 2534 - 2537
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; dichloro(cycloocta-1,5-diene)palladium(II) in water; tert-butyl alcohol T=95°C; Suzuki-Miyaura cross-coupling; 22 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 12 p. 3138 - 3141
反应条件
C45H59ClNPPd; potassium carbonate in water; tert-butyl alcohol T=85°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2013 , vol. 15, # 10 p. 2534 - 2537
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in water; toluene T=85°C; Suzuki-Miyaura cross-coupling reaction; 22 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2011 , vol. 13, # 15 p. 3956 - 3959
反应条件
palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; toluene T=85°C; Suzuki-Miyaura cross-coupling reaction; 22 h; Inert atmosphere;
参考文献
Molander, Gary A.; Shin, Inji
Organic Letters, 2011 , vol. 13, # 15 p. 3956 - 3959
