4-丙酰氧基-4-苯基-N-甲基哌啶合成路线 (共 2 条)
反应条件
dihydrogen peroxide in methanol 1.) room temperature, 48 h, 2.) heating, 2 h; other reagent: m-chloroperbenzoic acid;
参考文献
Groutas, W.C.; Essawi, M.; Portoghese, P.S.
Synthetic Communications, 1980 , vol. 10, # 7 p. 495 - 502
反应条件
1: aq. hydrogen peroxide / methanol / 1.) room temperature, 48 h, 2.) heating, 2 h; other reagent: m-chloroperbenzoic acid
2: 1.) trifluoroacetic anhydride / 1.) methylene chloride, room temperature, 1 h; heating, 20 min, 2.) water, room temperature, 1 h
View Scheme
参考文献
Groutas, W.C.; Essawi, M.; Portoghese, P.S.
Synthetic Communications, 1980 , vol. 10, # 7 p. 495 - 502