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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1,4-二苯基三唑
合成路线
（共 34 条）
591-50-4
碘苯
+
536-74-3
苯乙炔
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
copper(l) iodide; sodium azide; sodium L-ascorbate; N-methyl-2-(methylamino)ethylamine in water; dimethyl sulfoxide T=60°C; Huisgen cycloaddition; 15 h; Inert atmosphere;
参考文献
Potratz, Stefanie; Mishra, Amaresh; Baeuerle, Peter
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 683 - 692
536-74-3
苯乙炔
+
622-37-7
叠氮
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
[(ICy)2Cu]PF6 T=20°C; Huisgen cycloaddition; 0.0833333 h; Product distribution / selectivity;
参考文献
Oezcubukcu, Salih; Ozkal, Erhan; Jimeno, Cirll; Pericas, Miquel A.
Organic Letters, 2009 , vol. 11, # 20 p. 4680 - 4683
536-74-3
苯乙炔
+
98-80-6
苯硼酸
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
1: 3,4,5-trimethoxyphenylboronic acid With sodium azide in water T=20°C; 2: phenylacetylene in water T=20°C; 4 h; Concentration;
参考文献
Kaboudin, Babak; Mostafalu, Ramin; Yokomatsu, Tsutomu
Green Chemistry, 2013 , vol. 15, # 8 p. 2266 - 2274
536-74-3
苯乙炔
+
74497-02-2
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
sodium azide; tert.-butylnitrite; CuNPs/C in water T=70°C; 3 h;
参考文献
Alonso, Francisco; Moglie, Yanina; Radivoy, Gabriel; Yus, Miguel
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3208 - 3214
369-57-3
四氟硼酸重氮苯盐
+
536-74-3
苯乙炔
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
sodium azide; CuNPs/C in water T=70°C; 2 h;
参考文献
Alonso, Francisco; Moglie, Yanina; Radivoy, Gabriel; Yus, Miguel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 18 p. 6385 - 6395
108-86-1
溴代苯
+
536-74-3
苯乙炔
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
copper(l) iodide; sodium azide; sodium L-ascorbate; N-methyl-2-(methylamino)ethylamine in water; dimethyl sulfoxide T=95°C; Huisgen cycloaddition; 15 h; Inert atmosphere;
参考文献
Potratz, Stefanie; Mishra, Amaresh; Baeuerle, Peter
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 683 - 692
591-50-4
碘苯
+
112614-96-7
→
反应条件
20034-95-1
+
13148-78-2
1,4-二苯基三唑
反应条件
potassium carbonate; L-proline; copper(l) chloride in dimethyl sulfoxide T=160°C; 0.5 h; Microwave irradiation; regioselective reaction;
参考文献
Liu, Yuxiu; Yan, Wuming; Chen, Yunfeng; Petersen, Jeffrey L.; Shi, Xiaodong
Organic Letters, 2008 , vol. 10, # 23 p. 5389 - 5392
75918-91-1
→
反应条件
15765-06-7
+
13148-78-2
1,4-二苯基三唑
+
75918-79-5
反应条件
sodium hydrogencarbonate in dimethyl sulfoxide T=60 - 100°C; 2 h;
参考文献
Bedford, C. D.; Bruckmann, E. M.; Smith, P. A. S.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 679 - 686
108-86-1
溴代苯
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; tetrabutylammomium bromide; potassium carbonate in methanol; water T=20 - 150°C; Suzuki-Miyaura Coupling; 0.666667 h; Microwave irradiation;
参考文献
Kim, Taejung; Song, Jung Ho; Jeong, Kyu Hyuk; Lee, Seokjoon; Ham, Jungyeob
European Journal of Organic Chemistry, 2013 , # 19 p. 3992 - 3996
→
反应条件
13148-78-2
1,4-二苯基三唑
反应条件
1: ethynyl trifluoroborate potassium salt; iodobenzene With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in dimethyl sulfoxide T=40°C; 1 h; 2: diazoaminobenzene in water; dimethyl sulfoxide T=60°C; Sonogashira Cross-Coupling; 3 h; Reagent/catalystTemperatureTime;
参考文献
Song, Jung Ho; Choi, Pilju; Lee, Seung Eon; Jeong, Kyu Hyuk; Kim, Taejung; Kang, Ki Sung; Choi, Yong Soo; Ham, Jungyeob
European Journal of Organic Chemistry, 2013 , # 28 p. 6249 - 6253
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