in tetrahydrofuran byproducts: LiOSi(CH3)3; a suspn. of germatrane in THF was treated with an excess of n-BuLi in n-hexane at room temp. for 4 h; evap., filtered;
参考文献
Karlov, Sergey S.; Shutov, Pavel L.; Akhmedov, Novruz G.; Seip, Markus A.; Lorberth, Joerg; Zaitseva, Galina S.
Journal of Organometallic Chemistry, 2000 , vol. 598, # 2 p. 387 - 394
