1: triisopropylsilyl chloride; Trimethylene glycol With sodium hydride in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: triisopropylsilyl chloride in tetrahydrofuran Inert atmosphere;
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Park, Young Sam; Grove, Charles I.; Gonzalez-Lopez, Marcos; Urgaonkar, Sameer; Fettinger, James C.; Shaw, Jared T.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3730 - 3733
1: 4-methoxy pyridine With lithium diisopropyl amide in tetrahydrofuran; n-heptane; ethylbenzene T=-25°C; 0.5 h; 2: triisopropylsilyl chloride in tetrahydrofuran; n-heptane; ethylbenzene T=-25 - 20°C; 16.25 h;
参考文献
Brotherton-Pleiss, Christine E.; Caroon, Joan Marie; Lopez-Tapia, Francisco Javier
Patent: US2010/160388 A1, 2010 ;
Location in patent: Page/Page column 50-51 ;
US 20100160388 A1
1: With N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=20°C; 12 h; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran Inert atmosphere;
参考文献
Murakami, Kei; Yorimitsu, Hideki; Oshima, Koichiro
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1415 - 1417
