2,6-二-叔-丁基-4-甲基-4-叔-丁基过氧-2,5-环己二烯酮合成路线 (共 11 条)
反应条件
Rh2(cap)4 in water; 1,2-dichloro-ethane T=40°C; 0.75 h; chemoselective reaction;
参考文献
Ratnikov, Maxim O.; Farkas, Linda E.; McLaughlin, Emily C.; Chiou, Grace; Choi, Hojae; El-Khalafy, Sahar H.; Doyle, Michael P.
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2585 - 2593
反应条件
tert.-butylhydroperoxide; phosphomolybdic acid in acetic acid T=30°C; 3 h;
参考文献
Shimizu, Masao; Orita, Hideo; Hayakawa, Takashi; Watanabe, Yoshihito; Takehira, Katsuomi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2583 - 2584
反应条件
in ethyl acetate T=50°C; 8.5 h;
参考文献
Ochiai, Masahito; Nakanishi, Akinobu; Yamada, Akiko
Tetrahedron Letters, 1997 , vol. 38, # 22 p. 3927 - 3930
反应条件
[Ti(tert-butoxide)4] in benzene T=20°C;
参考文献
Stepovik; Gulenova; Martynova; Mar'Yasin; Cherkasov
Russian Journal of General Chemistry, 2008 , vol. 78, # 2 p. 266 - 276
反应条件
phosphomolybdic acid in acetic acid T=30°C; 3 h; other catalysts; other substrates; Product distribution;
参考文献
Shimizu, Masao; Orita, Hideo; Hayakawa, Takashi; Watanabe, Yoshihito; Takehira, Katsuomi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2583 - 2584
反应条件
1: oxygen; aq.-ethanolic KOH 2: NaI; acetic acid View Scheme
参考文献
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
反应条件
1: NaI; acetic acid View Scheme
参考文献
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
参考文献
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
反应条件
in dichloromethane T=-78 - 25°C; other radicals, var. reaction times; Product distribution;
参考文献
Pryor, William A.; Gu, Jen-tau; Church, Daniel F.
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 185 - 189
反应条件
(i) (irradiation), (ii) /BRN= 1911640/; Multistep reaction;
参考文献
Bartlett,P.D.; Lahav,M.
Israel Journal of Chemistry, 1972 , vol. 10, p. 101 - 109