131543-46-9合成路线 （共 480 条）
参考文献
Karmas; Spoerri
Journal of the American Chemical Society, 1952 , vol. 74, p. 1580,1582
Full Text Show Details
Jones
Journal of the American Chemical Society, 1949 , vol. 71, p. 78,79, 80
参考文献
Am. Cyanamid Co.
Patent: US2805223 , 1955 ;
反应条件
1: With 1,2,3-Benzotriazole in methanol; water T=2 - 20°C; 4 h; 2: With sodium tetrahydroborate in methanol; water T=20°C; 2 h; 3: With potassium hydroxide in water Product distribution / selectivity;
参考文献
US2006/217548 A1, ;
Page/Page column 3; 5 ;
反应条件
potassium carbonate in acetonitrile
参考文献
US2005/112066 A1, ;
Page/Page column 6 ;
反应条件
in water; acetonitrile
参考文献
Tetrahedron Letters, , vol. 21, p. 335 - 338
反应条件
1: With 1,2,3-Benzotriazole in methanol; water T=2 - 20°C; 3 h; 2: With sodium tetrahydroborate in methanol; water T=20°C; 2 h; 3: With potassium hydroxide in water Product distribution / selectivity;
参考文献
US2006/217548 A1, ;
Page/Page column 3; 5 ;
反应条件
in methanol Yield given;
参考文献
Acta Chemica Scandinavica, , vol. 52, # 12 p. 1402 - 1404
反应条件
sodium hydroxide in water T=100°C; internal Cannizzaro reaction; 0.166667 h;
参考文献
Schramm, Christian; Rinderer, Beate
Analytical Chemistry, 2000 , vol. 72, # 23 p. 5829 - 5833
反应条件
1: formaldehyd; ammonia; 1-amino-2-propene in water T=25°C; 1 h; 2: ethane-1,2-dial; ammonia T=25°C; 1 h;
参考文献
JP2005/82551 A, ;
Page 5 ;
反应条件
in ethanol; water 18 h;
参考文献
UCB PHARMA S.A.; BUeRLI, Roland; HAUGHAN, Alan, Findlay; MACK, Stephen, Robert; PERRY, Benjamin, Garfield; RAPHY, Gilles; SAVILLE-STONES, Elizabeth, Anne
Patent: WO2010/52448 A2, 2010 ;
Location in patent: Page/Page column 73 ;
WO 2010/052448 A2
