131543-46-9合成路线 (共 480 条)
反应条件
ammonium acetate in methanol; water 5 h; Heating;
参考文献
Matsuoka, Yuki; Ishida, Yasuhiro; Sasaki, Daisuke; Saigo, Kazuhiko
Tetrahedron, 2006 , vol. 62, # 34 p. 8199 - 8206
参考文献
Radziszewski
Chemische Berichte, 1882 , vol. 15, p. 2706
Chemische Berichte, 1883 , vol. 16, p. 487
反应条件
ammonium hydroxide in methanol
参考文献
Xu, Yuelian; Han, Bingsong; Wang, Zhe-Qing; Shaw, Kenneth R.; Chenard, Bertrand L.; Maynard, George; Xie, Linghong
Organic Process Research and Development, 2007 , vol. 11, # 4 p. 716 - 720
反应条件
1: ethane-1,2-dial; aniline in methanol T=20°C; 0.166667 h; 2: formaldehyd; ammonium chloride in methanol; water 1 h; Reflux; 3: With phosphoric acid in methanol; water 8 h; Reflux;
参考文献
Micksch, Maik; Strassner, Thomas
European Journal of Inorganic Chemistry, 2012 , # 35 p. 5872 - 5880
反应条件
1: formaldehyd; aniline in methanol T=20°C; 2: ethane-1,2-dial With ammonium chloride in methanol T=65°C; 3: With phosphoric acid in methanol T=65°C;
参考文献
Meyer, Dirk; Strassner, Thomas
Journal of Organic Chemistry, 2011 , vol. 76, # 1 p. 305 - 308
参考文献
Hollstein, Ulrich; Krisov, Galen E.
Organic Magnetic Resonance, 1980 , vol. 14, # 4 p. 300 - 304
反应条件
ammonium hydroxide in ethanol; water T=0 - 20°C;
参考文献
GTX, INC.; UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION; DALTON, James, T.; MILLER, Duane, D.; AHN, Sunjoo; CHEN, Jianjun; DUKE, Charles; LI, Chien-ming; LI, Wei; LU, Yan; WANG, Zhao
Patent: WO2011/109059 A1, 2011 ;
Location in patent: Paragraph 0041; 00356 ;
反应条件
ammonium acetate in methanol; water 5 h; Heating;
参考文献
Matsuoka, Yuki; Ishida, Yasuhiro; Sasaki, Daisuke; Saigo, Kazuhiko
Tetrahedron, 2006 , vol. 62, # 34 p. 8199 - 8206
反应条件
in methanol; water T=20°C; 3 h;
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
sodium tetrahydroborate in ethanol T=-10°C; 2 h;
参考文献
Chuburu, Francoise; Tripier, Raphael; Le Baccon, Michel; Handel, Henri
European Journal of Organic Chemistry, 2003 , # 6 p. 1050 - 1055