131543-46-9合成路线 （共 480 条）
反应条件
in water T=80 - 90°C; 1 h;
参考文献
Tayebee, Reza; Esmaei, Rezaei-Seresht; Behrooz, Maleki
Letters in Organic Chemistry, 2012 , vol. 9, # 3 p. 183 - 191
反应条件
hydrogenchloride; potassium hydroxide; sodium methylate in methanol; ethanol; ammonia; water; carbon
参考文献
Ciba-Geigy Corporation
Patent: US4011261 A1, 1977 ;
反应条件
sodium hydroxide; hydroxylammonium sulphate in water a.) 90-95 deg C, b.) 25 deg C, overnight;
参考文献
Park, Dennis J.; Stern, Alfred G.; Willer, Rodney L.
Synthetic Communications, 1990 , vol. 20, # 18 p. 2901 - 2906
反应条件
hydroxylamine hydrochloride; hydrazine hydrate in water 4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Harada, Katsumasa; Oda, Mizuho; Matsushita, Akio; Shirai, Masashi
Synlett, 1998 , # 4 p. 431 - 433
参考文献
Wittenberg; Meyer,V.
Chemische Berichte, 1883 , vol. 16, p. 502
反应条件
sodium ethanolate Abdampfen der mit Wasser versetzten Mischung und Ansaeuern mit Salzsaeure;
参考文献
Hinsberg
Chemische Berichte, 1912 , vol. 45, p. 2417
反应条件
phosphoric acid; ammonium chloride T=90 - 95°C; 0.166667 h; pH 2;
参考文献
Gridnev; Mihaltseva
Synthetic Communications, 1994 , vol. 24, # 11 p. 1547 - 1555
反应条件
water und anschliessenden Behandeln mit Benzolsulfonylchlorid und wss.NaOH;
参考文献
Bengelsdorf
Journal of the American Chemical Society, 1953 , vol. 75, p. 3138
反应条件
ammonium hydroxide in ethanol; water T=0 - 20°C;
参考文献
Chen, Jianjun; Wang, Zhao; Li, Chien-Ming; Lu, Yan; Vaddady, Pavan K.; Meibohm, Bernd; Dalton, James T.; Miller, Duane D.; Li, Wei
Journal of Medicinal Chemistry, 2010 , vol. 53, # 20 p. 7414 - 7427
反应条件
hydrogenchloride in water T=80 - 90°C; pH=1; 1 h;
参考文献
Russian Chemical Bulletin, , vol. 54, # 3 p. 691 - 704
