131543-46-9合成路线 (共 480 条)
反应条件
1: methyl 3-amino-benzoate; ethane-1,2-dial in methanol; water T=20°C; 18 h; 2: formaldehyd With ammonium chloride in methanol; water 1 h; Reflux; 3: With hydrogenchloride in methanol; water 5 h; Reflux;
参考文献
Gilfillan, Lynne; Blair, Adele; Morris, Brian J.; Pratt, Judith A.; Schweiger, Lutz; Pimlott, Sally; Sutherland, Andrew
MedChemComm, 2013 , vol. 4, # 7 p. 1118 - 1123
反应条件
acetic acid in water T=5°C; 1 h;
参考文献
Nourmohammadian, Farahnaz; Gholami, Mahnaz Davoudzadeh
Helvetica Chimica Acta, 2012 , vol. 95, # 9 p. 1548 - 1555
反应条件
acetic acid in methanol; water
参考文献
Gallucci, Robert R.
Journal of Chemical & Engineering Data, 1982 , vol. 27, # 2 p. 217 - 219
参考文献
McElvain et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 5736,3737
Full Text Show Details
Eisenberg; Gurin
Journal of the American Chemical Society, 1951 , vol. 73, p. 4440,4442
反应条件
hydrogenchloride; hydroxylamine hydrochloride in methanol; water T=20°C; 20 h;
参考文献
Bartza, Susan; Blumenroedera, Bettina; Kernb, Anika; Fleckensteinb, Julia; Frohnapfelb, Sabine; Schatz, Juergen; Wagnerb, Alexander
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2009 , vol. 64, # 6 p. 629 - 638
反应条件
water; toluene-4-sulfonic acid Entfernen des entstehenden Wassers;
参考文献
Sprung; Guenther
Journal of the American Chemical Society, 1951 , vol. 73, p. 1884
反应条件
lithium perchlorate; toluene-4-sulfonic acid in water; toluene 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martinez-Bernhardt, Rolando; Castro, Peter P.; Godjoian, Gayane; Gutierrez, Carlos G.
Tetrahedron, 1998 , vol. 54, # 31 p. 8919 - 8932
参考文献
Wilcox,C.F. et al.
Journal of the American Chemical Society, 1972 , vol. 94, # 7 p. 2532 - 2533
参考文献
Dakin; Dudley
Journal of Biological Chemistry, 1913 , vol. 15, p. 137
Full Text Show Details
Curtius
Journal fuer Praktische Chemie (Leipzig), 1917 , vol. <2> 95, p. 211
参考文献
Ferruti,P. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2984 - 2985