131543-46-9合成路线 (共 480 条)
反应条件
in ethanol; water 8 h;
参考文献
IDEMITSU KOSAN CO., LTD.
Patent: EP1749823 A1, 2007 ;
Location in patent: Page/Page column 30 ;
反应条件
ammonium hydroxide; water in ethanol T=0 - 20°C;
参考文献
Xiao, Min; Ahn, Sunjoo; Wang, Jin; Chen, Jianjun; Miller, Duane. D.; Dalton, James T; Li, Wei
Journal of Medicinal Chemistry, 2013 , vol. 56, # 8 p. 3318 - 3329
反应条件
sodium hydroxide in methanol; water T=-20°C; 2 h; Yield given;
参考文献
Baertschi; Dorman; Occolowitz; Spangle; Collins; Wildfeuer; Lorenz
Journal of Pharmaceutical Sciences, 1993 , vol. 82, # 6 p. 622 - 626
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 9 p. 3608 - 3615
反应条件
und Behandeln des Reaktionsprodukts mit wss.NaOH;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 14,18
Journal of the American Chemical Society, , vol. 74, p. 3877,3881
反应条件
phosphoric acid; dihydrogen peroxide; urea in methanol; water
参考文献
Kenegafuchi Kagaku Kogyo Kabushiki Kaisha
Patent: US5110944 A1, 1992 ;
参考文献
Herrmann,J.L. et al.
Tetrahedron Letters, 1973 , p. 4711 - 4714
反应条件
sodium hydroxide; hydroxylamine hydrochloride 1.) 0-5 deg C, 10 min, 2.) 90-100 deg C, 5 h;
参考文献
Martinez, Henry; Zheng, Zhaoyun; Dolbier Jr., William R.
Journal of Fluorine Chemistry, 2012 , vol. 143, p. 112 - 122,11
反应条件
in water; isopropyl alcohol T=80°C; 2 h;
参考文献
METHYLGENE, INC.
Patent: WO2005/30704 A1, 2005 ;
Location in patent: Page/Page column 222 ;
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 9 p. 612 - 616