131543-46-9合成路线 （共 480 条）
反应条件
1: isobutyraldehyde With ammonia in methanol; water T=25°C; 1 h; 2: ethane-1,2-dial With ammonia in methanol; water T=25°C; 2 h; Product distribution / selectivity;
参考文献
Nippon Synthetic Chemical Industry Co., Ltd.
Patent: JP2005/82570 A, 2005 ;
Location in patent: Page/Page column 5 ;
参考文献
Ljubawin
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1875 , vol. 7, p. 254
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Wyss
Chemische Berichte, 1876 , vol. 9, p. 1544
Chemische Berichte, 1877 , vol. 10, p. 1366
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Debus
Justus Liebigs Annalen der Chemie, 1858 , vol. 107, p. 199
反应条件
1: formaldehyd; ammonia; ethanolamine in water T=25°C; 1 h; 2: ethane-1,2-dial; ammonia T=25°C; 1 h; Product distribution / selectivity;
参考文献
Nippon Synthetic Chemical Industry Co., Ltd.
Patent: JP2005/82551 A, 2005 ;
Location in patent: Page 4 ;
反应条件
ammonia in water 2 h; Product distribution / selectivity;
参考文献
Nippon Synthetic Chemical Industry Co., Ltd.
Patent: JP2005/82551 A, 2005 ;
Location in patent: Page/Page column 5 ;
参考文献
Sankio Chemical Co., Ltd.
Patent: EP1186596 A1, 2002 ;
Location in patent: Page 8 ;
反应条件
1: acetamidrazone hydrochloride With sodium hydrogencarbonate in diethyl ether T=20°C; 0.25 h; 2: ethane-1,2-dial in diethyl ether 3 h; Further stages.;
参考文献
Courcot, Blandine; Tran, Diem Ngan; Fraisse, Bernard; Bonhomme, Francois; Marsura, Alain; Ghermani, Nour Eddine
Chemistry - A European Journal, 2007 , vol. 13, # 12 p. 3414 - 3423
反应条件
sodium acetate in ethanol; water 0.5 h; Heating;
参考文献
Kobayashi, Tomoshige; Kobayashi, Sayuri
European Journal of Organic Chemistry, 2002 , # 13 p. 2066 - 2073
反应条件
toluene-4-sulfonic acid T=20°C; 0.5 h;
参考文献
He, Jingyu; Xin, Hongxing; Yan, Hong; Song, Xiuqing; Zhong, Rugang
Helvetica Chimica Acta, 2011 , vol. 94, # 1 p. 159 - 162
反应条件
ammonium acetate in toluene T=70°C; Inert atmosphere;
参考文献
Aspin, Sam; Lopez-Suarez, Laura; Larini, Paolo; Goutierre, Anne-Sophie; Jazzar, Rodolphe; Baudoin, Olivier
Organic Letters, 2013 , vol. 15, # 19 p. 5056 - 5059
反应条件
sodium hydroxide in methanol; water T=-35 - 20°C;
参考文献
Gerritsma, David A.; Brindle, Ian D.; Jones, Timothy R.B.; Capretta, Alfredo
Journal of Labelled Compounds and Radiopharmaceuticals, 2003 , vol. 46, # 3 p. 243 - 253
