反应条件
1: 97 percent / LiAlH4 / tetrahydrofuran / 0 °C 2: 93 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 18 h / 0 °C 3: 80 percent / LiAlH4 / tetrahydrofuran / 8 h / Ambient temperature 4: 10percent aq. HCl / tetrahydrofuran 5: pyridinium chlorochromate, 3-Angstroem molecular sieves / CH2Cl2 / Ambient temperature View Scheme
参考文献
Mash, Eugene A.; Arterburn, Jeffrey B.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 885 - 888