4-甲氧基-N-亚磺酰基苯胺合成路线 （共 6 条）
反应条件
hydrogenchloride; thionyl chloride in benzene Heating;
参考文献
Al-Ajely, Mohammed S.; Al-Rawi, Jasim M. A.; Elvidge, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1575 - 1578
反应条件
in dichloromethane 1.) -40 deg C, 2.) 20 deg C, 0.5 h;
参考文献
Kim, Yong Hae; Shin, Jai Moo
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3821 - 3824
反应条件
triphenylphosphine in tetrahydrofuran under N2, mixt. of Fe-complex, 4-MeOC6H4NSO and PPh3 (molar ratio 1:1:2) in THF were stirred for 1-4 h at room temp.; solvent removed under reduced pressure, chromd. on alumina column (CH2Cl2), recrystd. from CH2Cl2-hexane; elem. anal.;
参考文献
Ashton, Henry C.; Manning, A. R.
Inorganic Chemistry, 1983 , vol. 22, p. 1440 - 1445
参考文献
Baltas, Michel; Cazaux, Louis; Slic, Arnaud De; Corrichons, Liliane; Tisnes, Pierre
Journal of Chemical Research, Miniprint, 1988 , # 9 p. 2236 - 2261
反应条件
triphenylphosphine in tetrahydrofuran
under N2, mixt. of Fe-complex, 4-MeOC6H4NSO and PPh3 (molar ratio 1:1:2) in THF were stirred for 1-4 h at room temp.; solvent removed under reduced pressure, chromd. on alumina column (CH2Cl2), recrystd. from CH2Cl2-hexane; elem. anal.;
参考文献
Ashton, Henry C.; Manning, A. R.
Inorganic Chemistry, 1983 , vol. 22, p. 1440 - 1445
反应条件
5V/SiO2-300 in n-heptane
T=98°C; 12 h; Inert atmosphere;
参考文献
Zhizhko, Pavel A.; Zhizhin, Anton A.; Zarubin, Dmitry N.; Ustynyuk, Nikolai A.; Lemenovskii, Dmitry A.; Shelimov, Boris N.; Kustov, Leonid M.; Tkachenko, Olga P.; Kirakosyan, Gayane A.
Journal of Catalysis, 2011 , vol. 283, # 1 p. 108 - 118
