(三甲基硅基)甲基氯化镁合成路线 （共 130 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in tetrahydrofuran; diethyl ether
参考文献
Shimizu, Ryo; Egami, Hiromichi; Hamashima, Yoshitaka; Sodeoka, Mikiko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 19 p. 4577 - 4580
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
16 h; Heating; Yield given. Yields of byproduct given;
参考文献
Wong, Ken-Tsung; Ni, Zhi-Jie; Luh, Tien-Yau
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3113 - 3116
反应条件
lithium 1-dimethylaminonaphthalenide
1.) diethyl ether/ THF, -78 deg C, 3 h, 2.) -78 deg C; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Fernandez-Simon, Jose L.; Concellon, Jose M.; Yus, Miguel
Tetrahedron Letters, 1989 , vol. 30, # 43 p. 5927 - 5928
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether
T=20°C; Kumada-Tamao-Corriu coupling;
参考文献
Uenishi, Jun'ichi; Iwamoto, Takuya; Ohmi, Masashi
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1237 - 1240
反应条件
in diethyl ether
2 h; Ambient temperature;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 71 - 88
反应条件
cerium(III) chloride
参考文献
Lee, Thomas V.; Porter, John R.; Roden, Frances S.
Tetrahedron Letters, 1988 , vol. 29, # 39 p. 5009 - 5012
反应条件
ethylmagnesium bromide; copper(I) bromide
1.) ether, -10 deg C 2.) ether, -10 deg C to R.T., 26 h; Yield given. Multistep reaction;
参考文献
Foulon, J. P.; Bourgain-Commercon, M.; Normant, J. F.
Tetrahedron, 1986 , vol. 42, # 5 p. 1389 - 1398
反应条件
n-butyllithium; bis(1,3-diphenylphosphinopropane) nickel(II) chloride
1.) THF, hexane, 0 deg C, 10 min, 2.) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Organ, Michael G.; Murray, Aaron P.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1523 - 1526
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
15 h; Ambient temperature;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Okamoto, Yasuo; Kumada, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 44 p. 4449 - 4452
反应条件
copper(l) iodide in tetrahydrofuran
T=-40°C; 1.5 h;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
