反应条件
1: NaBH4 / ethanol
2: pyridine
3: 90percent HCOOH
4: SOCl2
5: 39 percent / Et3N / CH2Cl2
6: H2O, OH(1-)
7: 71 percent / 1percent TFAA / toluene / -20 °C
8: pyridine
9: LiBH4 / ethanol
10: 3N HCl / H2O; dioxane
View Scheme
参考文献
Sakamoto, Akio; Yamamoto, Yukio; Oda, Jun'ichi
Journal of the American Chemical Society, 1987 , vol. 109, # 23 p. 7188 - 7189
