1,1,1,3,3,3-六氟异丙基甲基醚合成路线 (共 14 条)
反应条件
KHF2 in 1-methyl-pyrrolidin-2-one; water T=150°C; 3 h; Product distribution / selectivity;
参考文献
Daikin Industries, Ltd.
Patent: EP2025663 A1, 2009 ;
Location in patent: Page/Page column 12 ;
反应条件
KHF2; water in 1-methyl-pyrrolidin-2-one T=130 - 150°C; 6 h; Product distribution / selectivity;
参考文献
Daikin Industries, Ltd.
Patent: EP2025663 A1, 2009 ;
Location in patent: Page/Page column 10-11 ;
反应条件
water in dimethyl sulfoxide T=150°C; 3 h; Product distribution / selectivity;
参考文献
EP2025663 A1, ;
Page/Page column 9-10 ;
反应条件
sulfuric acid in bis [2-(2-methoxyethoxy)ethyl] ether; water T=100°C; P=3150.32 Torr; pH=1; 2 h; Product distribution / selectivity;
参考文献
EP2025663 A1, ;
Page/Page column 9 ;
反应条件
water in acetonitrile T=150°C; 3 h; Product distribution / selectivity;
参考文献
EP2025663 A1, ;
Page/Page column 9-10 ;
反应条件
potassium hydroxide; water T=50°C; 2 h;
参考文献
EP2039675 A1, ;
Page/Page column 7-8 ;
反应条件
in bis [2-(2-methoxyethoxy)ethyl] ether; water T=80°C; P=2625.26 Torr; 2 h; Product distribution / selectivity;
参考文献
EP2025663 A1, ;
Page/Page column 9 ;
反应条件
potassium hydroxide in water T=68 - 70°C; Etherification;
参考文献
Nielsen, Gunnar D.; Abraham, Michael H.; Hansen, Lea F.; Hammer, Maria; Cooksey, Christopher J.; Andonian-Haftvan, Jenik; Alarie, Yves
Archives of Toxicology, 1996 , vol. 70, # 6 p. 319 - 328
反应条件
in water T=75°C; 3 h; Autoclave; Product distribution / selectivity;
参考文献
US2010/312019 A1, ;
Page/Page column 4 ;
反应条件
in methanol 2 h; Heating;
参考文献
Zapevalov, A. Ya.; Filyakova, T. I.; Kolenko, I. P.; Peschanskii, N. V.; Kodess, M. I.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 11 p. 2267 - 2273