15,17,19,21-三十六碳四炔合成路线 （共 3 条）
反应条件
N,N,N',N,-tetramethylethylenediamine; oxygen; copper(l) chloride in tetrahydrofuran 6 h; Ambient temperature;
参考文献
Okada, S.; Matsuda, H.; Nakanishi, H.; Kato, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 189, # 1 p. 57 - 63
反应条件
1: 45 percent / 2-aminopropane, cuprous chloride, NH2OH*HCl / ethanol / 2 h / Ambient temperature 2: 85 percent / potassium hydroxide / benzene / 5 h / Heating 3: 63 percent / cuprous chloride, N,N,N',N'-tetramethylethylenediamine, oxygen / tetrahydrofuran / 6 h / Ambient temperature View Scheme
参考文献
Okada, S.; Matsuda, H.; Nakanishi, H.; Kato, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 189, # 1 p. 57 - 63
反应条件
1: 85 percent / potassium hydroxide / benzene / 5 h / Heating 2: 63 percent / cuprous chloride, N,N,N',N'-tetramethylethylenediamine, oxygen / tetrahydrofuran / 6 h / Ambient temperature View Scheme
参考文献
Okada, S.; Matsuda, H.; Nakanishi, H.; Kato, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 189, # 1 p. 57 - 63
