hydrazine hydrate; nickel in ethanol 2 h; Heating;

2: 95 percent / 20percent aq. KOH / ethanol / 48 h / Heating 3: thionyl chloride (SOCl2) / 1 h / Heating 4: AlCl3 / CH2Cl2 / 0.33 h / 0 °C 5: NaBH4 / CH2Cl2; methanol / 2 h / Ambient temperature 6: p-toluenesulfonic acid / toluene / 3 h / Heating 7: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 8: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: thionyl chloride (SOCl2) / 1 h / Heating 2: AlCl3 / CH2Cl2 / 0.33 h / 0 °C 3: NaBH4 / CH2Cl2; methanol / 2 h / Ambient temperature 4: p-toluenesulfonic acid / toluene / 3 h / Heating 5: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 6: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: NaBH4 / CH2Cl2; methanol / 2 h / Ambient temperature 2: p-toluenesulfonic acid / toluene / 3 h / Heating 3: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 4: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 2: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: p-toluenesulfonic acid / toluene / 3 h / Heating 2: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 3: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: AlCl3 / CH2Cl2 / 0.33 h / 0 °C 2: NaBH4 / CH2Cl2; methanol / 2 h / Ambient temperature 3: p-toluenesulfonic acid / toluene / 3 h / Heating 4: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 5: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

1: 95 percent / 20percent aq. KOH / ethanol / 48 h / Heating 2: thionyl chloride (SOCl2) / 1 h / Heating 3: AlCl3 / CH2Cl2 / 0.33 h / 0 °C 4: NaBH4 / CH2Cl2; methanol / 2 h / Ambient temperature 5: p-toluenesulfonic acid / toluene / 3 h / Heating 6: 32 percent / AgNO2, NaNO2, I2 / acetonitrile / 48 h / Ambient temperature 7: 94 percent / hydrazine monohydrate / Raney Ni / ethanol / 2 h / Heating View Scheme

Salmonella typhimurium TA98 in various solvent(s) T=37°C; Reduction; pH=7.5; Enzyme kinetics; Further Variations:Reagents;

Acetylation;