N-丁氧羰基-4-溴丙氨酸合成路线 （共 19 条）
反应条件
in toluene T=70°C; 15 h;
参考文献
Chankeshwara, Sunay V.; Chakraborti, Asit K.
Synthesis, 2006 , # 16 p. 2784 - 2788
反应条件
sodium hexamethyldisilazane in tetrahydrofuran; ethyl acetate
参考文献
Eli Lilly and Company
Patent: US6303816 B1, 2001 ;
反应条件
sodium hydroxide in hexane
反应条件
sodium hydroxide in hexane
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); tri-iso-propylsilanol; potassium hydroxide in water T=20°C; 14 h; Inert atmosphereGreen chemistry;
参考文献
Isley, Nicholas A.; Dobarco, Sebastian; Lipshutz, Bruce H.
Green Chemistry, 2014 , vol. 16, # 3 p. 1480 - 1488
反应条件
methanol; tris(acetonitrile)(tricarbonyl)molybdenum T=130°C; 0.25 h; Microwave irradiationInert atmosphere; chemoselective reaction;
参考文献
Nielsen, Simon Dalsgaard; Smith, Garrick; Begtrup, Mikael; Kristensen, Jesper L.
European Journal of Organic Chemistry, 2010 , # 19 p. 3704 - 3710
反应条件
trimethylsilylazide; 1-propanephosphonic acid cyclic anhydride; triethylamine in tetrahydrofuran Curtius rearrangement; 0.5 h; Reflux;
参考文献
Augustine, John Kallikat; Bombrun, Agnes; Mandal, Ashis Baran; Alagarsamy, Padma; Atta, Rajendra Nath; Selvam, Panneer
Synthesis, 2011 , # 9 art. no. Z17611SS, p. 1477 - 1483
反应条件
1: bis-[(trifluoroacetoxy)iodo]benzene / 1,2-dichloro-ethane / 0.03 h / |Molecular sieve; |Inert atmosphere 2: 1,2-dichloro-ethane / 1 h / 60 °C / |Molecular sieve; |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 14 p. 2172 - 2175
反应条件
in 1,2-dichloro-ethane T=60°C; 1 h; Molecular sieveInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 14 p. 2172 - 2175
