(3-甲基苯基)(4-硝基苯基)甲酮合成路线 (共 3 条)
反应条件
C57H43IP2Pd; potassium carbonate in 1,4-dioxane T=90°C; carbonylative Suzuki coupling; P=3750.38 Torr; 12 h; Autoclave;
参考文献
Kaganovsky, Luba; Gelman, Dmitri; Rueck-Braun, Karola
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 260 - 266
反应条件
bis(acetylacetonato) palladium; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4; cataCXium® AHI in toluene T=80°C; Suzuki-Miyaura Coupling; 16 h; Inert atmosphere;
参考文献
Bjerglund, Klaus M.; Skrydstrup, Troels; Molander, Gary A.
Organic Letters, 2014 , vol. 16, # 7 p. 1888 - 1891
反应条件
C4F9SO3H T=110°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 116, # 3 p. 1195 - 1208